Determination of Trace Amounts of Tin by Reversed-phase HPLC after Solid Phase Extraction-Preconcentration with XAD Resin Coated with N-Benzoyl-N-phenylhydroxylamine.
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چکیده
منابع مشابه
Determination of some trace metals by FAAS after solid-phase extraction with amberlite XAD-1180/TAN chelating resin.
A new chelating resin was synthesized by immobilizing 1-(2-thiazolylazo)-2-naphthol through the -N=N- group on Amberlite XAD-1180. The resin was used for the preconcentration of Cd(II), Co(II), Cu(II), Mn(II), Ni(II), and Pb(II) ions and their determination by flame atomic absorption spectrometry (FAAS). The influences of some analytical parameters, such as the pH, volume of the sample, flow ra...
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A solid-phase extraction (SPE) method for sample clean-up and preconcentration followed by reversed-phase high-performance liquid chromatography (RP-HPLC) with uv detection is reported for determination of polycyclic aromatic hydrocarbons (PAHs) in the caspian seawater. A good resolution was obtained using acetonitrile:water (40:60) as mobile-phase for separation of these compounds. The eff...
متن کاملReview of preconcentration and solid phase extraction for the determination of trace Lead
Spectrometric techniques for the analysis of trace lead have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, and considers the features of the application with several spectrometric techniques. The use of an appropriate sample handling technique is a...
متن کاملReview of preconcentration and solid phase extraction for the determination of trace Lead
Spectrometric techniques for the analysis of trace lead have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, and considers the features of the application with several spectrometric techniques. The use of an appropriate sample handling technique is a...
متن کاملSolid Phase Extraction of Ultra Trace Amounts of Ni2+ by Dimethylglyoxime (DMG) Immobilized on Column
A column of alumina modified with sodium dodecyl sulfate (SDS) and dimethylglyoxime (DMG) was prepared for the preconcentration of trace nickel from water samples for flame atomic absorption spectrometry (FAAS) determinations. Under optimized conditions (pH=7.0; flow rate: 20 mlmin-1) nickel was retained on the column. The nickel collected on the column was eluted with 5 mL of 1 M nitric ac...
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ژورنال
عنوان ژورنال: NIPPON KAGAKU KAISHI
سال: 2001
ISSN: 0369-4577
DOI: 10.1246/nikkashi.2001.567